employee from 01.01.2010 until now
Krasnodar,, Krasnodar, Russian Federation
employee
employee from 01.01.2000 until now
Russian Federation
employee
FSBSI North Caucasus Federal Scientific Center of Horticulture, Viticulture, Winemaking (nauchnyy sotrudnik)
employee
VAK Russia 4.1.1
VAK Russia 4.1.2
VAK Russia 4.1.3
VAK Russia 4.1.4
VAK Russia 4.1.5
VAK Russia 4.2.1
VAK Russia 4.2.2
VAK Russia 4.2.3
VAK Russia 4.2.4
VAK Russia 4.2.5
VAK Russia 4.3.5
UDC 663.241
The aim of the study is to establish the effect of oak extract and caramel color on the quantitative and qualitative content of phenolic and furan compounds by adding these auxiliary agents in different concentrations to cognac distillate. The basis of the experiment was the creation of solutions of young or aged cognac distillates with the addition of caramel color, oak extract and bringing the resulting solutions to a volume fraction of ethyl alcohol of 40 %. The color was added according to visual control until the usual color of the cognac was created. The resulting solutions were aged for at least 10 days, without access to oxygen. Then, studies were conducted to identify mass concentrations of phenolic and furan compounds. In the experiment with young cognac distillate, a tendency was monitored for the introduction of certain amounts of syringaldehyde (0.1–0.4 mg/dm3) and gallic acid (0.8–5.9 mg/dm3) by oak extract, depending on the dosage. The control sample of aged cognac distillate contained sinapic, coniferyl and syringaldehydes, vanillin, syringic and gallic acids (0.2–5.3 mg/dm3). When oak extract was added with increasing dosage to the aged distillate, the mass concentration of gallic acid increased significantly – from 1.9 to 5.3 mg/dm3. When adding sugar color, the appearance of 5-methylfurfural in the composition of cognac distillates was noted at a concentration of 1.7–2.8 mg/dm3 for young, 1.0–2.5 mg/dm3 for aged. With an increase in the dose of caramel color added to both young and aged cognac distillate, a decrease in the 5-methylfurfural/2-furfural ratio was observed from 3.8 to 2.3 and from 6.0 to 2.6, respectively.
oak wood, distillates, aging, phenolic substances, furan compounds, color, oak extract, quality
1. Oseledtseva IV. Sovershenstvovaniye metodiki kontrolya kachestva kon'yachnoy produktsii. Nauchnye trudy KubGTU. 2016;(14):472–480. (In Russ.). EDN: https://elibrary.ru/ZHJRVZ.
2. Belkin Yu.D. Obzor sovremennykh metodov identifikatsii kon'yakov i brendi, primenyayemykh v otechestvennoy i zarubezhnoy praktike. Tovaroved prodovol'stvennykh tovarov. 2016;(9):8-13. (In Russ.). EDN: https://elibrary.ru/WXKPUT.
3. Ageyeva NM, Avanes'yants RV. Sovremennaya tekhnologiya obrabotki sakharnogo kolera i sakharnogo siropa dlya proizvodstva kon'yakov. Plodovodstvo i vinogradarstvo Yuga Rossii. 2013;19(1):133-139. (In Russ.). EDN: https://elibrary.ru/PLVPRP.
4. Andriyevskaya DV, Zakharov MA, Ul'yanova EV, et al. Izucheniye vliyaniya sakharosoderzhaschego syr'ya na kachestvennye kharakteristiki kon'yakov. Polzunovskiy vestnik. 2021;(1):34-43. (In Russ.). DOI:https://doi.org/10.25712/ASTU.2072-8921.2021.01.005. EDN: https://elibrary.ru/OASTNI.
5. Skurikhin IM. Khimiya kon'yaka i brendi. Moskva: DeLi Print; 2005. 296 p. (In Russ.). EDN: https://elibrary.ru/QNGIUB.
6. Dubovskaya NI, Zolotareva MS, Panov AV, et al. Razrabotka tekhnologii polucheniya sukhogo ekstrakta kory duba. Terapevt. 2021;(1):38-45. (In Russ.). DOI:https://doi.org/10.33920/MED-12-2101-07. EDN: https://elibrary.ru/OPJDXO.
7. Kolesnov AYu, Tsimbalayev SR, Lamerdonova FKh. Primeneniye vysokoeffektivnoy zhidkostnoy khromatografii dlya issledovaniya kachestva vinodel'cheskoy produktsii: sovremennyye metodicheskiye podkhody. Analitika. 2021;11(6):458-465. (In Russ.). DOI:https://doi.org/10.22184/2227-572X.2021.11.6.458.465. EDN: https://elibrary.ru/CNRFJM.
8. Oseledtseva IV, Nachevnaya EV, Nazarenko MA. Vliyaniye biokataliza i termoliza pri aktivatsii dubovoy drevesiny na kinetiku ekstraktsii i dinamiku nakopleniya benzoynykh i korichnykh al'degidov v kon'yachnykh distillyatakh. Izvestiya vysshikh uchebnykh zavedeniy. Pishchevaya tekhnologiya. 2022;(6):55-60. (In Russ.). DOI:https://doi.org/10.26297/0579-3009.2022.6.7. EDN: https://elibrary.ru/JAXRTS.
9. Ivanchenko KV. Issledovaniye dinamiki perekhoda v kon'yachnyy spirt fenol'nykh i ekstraktivnykh veshchestv iz razlichnykh preparatov duba. Izvestiya sel'skokhozyaystvennoy nauki Tavridy. 2015;(2):92-97. (In Russ.). EDN: https://elibrary.ru/WFDTWN.
10. Yuan X, Zhou J, Baochun Zh, et al. Identification, quantitation and organoleptic contributions of furan compounds in brandy. Food Chemistry. 2023;412:135543. DOI:https://doi.org/10.1016/j.foodchem.2023.135543.
